Nevertheless, incomplete geopolymerisation is still observed in this sample. Figure 7 d illustrates a geopolymer sample with ratio S/L 1.75 and Na 2 SiO 3 /NaOH 1.5 and the maximum compressive strength (11.5 MPa) was obtained. For this mix design with Na 2 SiO 3 /NaOH more than 2.0, the geopolymer samples were unable to be prepared due to low ...
به خواندن ادامه دهیدThe raw mix was dry-homogenized. For the synthesis, we used finely ground limestone filler, with a maximum residue on the 200 μm sieve of 2% and of 20% on the 90 μm sieve. The clay, gypsum, and bauxite were previously crushed and ground in the planetary ball mill (Fritsch Pulverisette planetary ball mill, Idar-Oberstein, Germany).
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به خواندن ادامه دهیدwith a vibrating mill and mixed with 200 mg of IR grade KBr (around 1 % of pellet weight), a KBr pellet is formed. in the sample may no longer be apparent as it was found when using dry ashing. Separation with heavy-liquid shows the benefit of the treat-ment: see result of the top right spectra in comparison with the SRM Chrysotile (lower right).
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به خواندن ادامه دهیدsample, mix and grind to a fine powder. For very hard samples, add the sample first, grind, add KBr and then grind again. The sample must be very finely ground as in the Nujol mulling technique to reduce scattering losses and absorption band distortions. Take two stainless steel disks out of the desiccator. Place a piece of the precut cardboard ...
به خواندن ادامه دهیدfar‐infrared testing, high‐density polyethylene (HDPE) or diamond dust is suitable. For near‐ infrared analysis, CsI or KBr can be selected. You can prepare a KBr Pellet as follows: (a) The powder sample and KBr must be ground to reduce the …
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به خواندن ادامه دهیدForms powder, you can mix milligrams of the sample in KBr spectroscopic (150 mg) If you want to grind the fibers and sheets and prepare the sample equal to the powder can too. After preparation of ...
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به خواندن ادامه دهیدAn electrode mix paste obtainable by kneading the ... a block, it is preferably first pulverized. There are no particular restrictions on the pulverization method, but a jet mill, vibrating mill, hammer mill, or the like can be used. ... (hereinafter also referred to as "peak intensity ratio (R = I 1360 /I 1580) ") : A sample was mixed with KBr ...
به خواندن ادامه دهیدIt was found, that sample with weight ratio HAP: Alg = 2:1 and containing 4.0 wt% of C60 has the highest Young's modulus 429 MPa comparing with other determined samples.
به خواندن ادامه دهیدThe extract was centrifuged at 3000 rpm for 15 min and made up to 25 ml with 80% (v/v) acetone.The clear solution was transferred and the optical density was measured at 645 nm and 663 nm against ...
به خواندن ادامه دهیدA sample of 300 students and employees from a Quebec university was used for the validation of the questionnaire. Concerning the reliability of the instrument, the indices observed following the inter-rater agreement (Krippendorff's alpha) and the calculation of the coefficients for internal consistency (Cronbach's alpha) are satisfactory.
به خواندن ادامه دهیدIn order to penetrate into the nano range, high-performance mills such as the Planetary Micro Mill PULVERISETTE 7 premium line must be used. more information. Comminution of dog food. An effective sample preparation is essential for the subsequent analysis of dog food. New technologies and testing methods for example are helping manufacturers ...
به خواندن ادامه دهیدA ball mill mixer (Retsch MM400, Haan, Germany) and hydraulic pellet press machine (Perkin Elmer, Norwalk, USA) were used for sample preparation before analysis. Raman spectra of ingredients in the composition of adulterated dry soup mix are presented in Figure 1.
به خواندن ادامه دهیدThe dried samples were ground in a mill and sieved in a sieve shaker of particle size 300 m. ... (Shimadzu-8400S). The adsorbent was encapsulated with KBr spectroscopy grade and by introducing the mix in a piston's cell of a hydraulic pump with compression pressure 15KPa/cm2, the solid transluscent disk was obtained. The FTIR spectrum was ...
به خواندن ادامه دهیدSamples were mixed with KBr powder in a mass ratio of (20꞉80, sample꞉KBr), and then were ground and pressed into a sheet for analysis. The X-Day diffraction (XRD) patterns of samples were obtained with a Mini Flex (Rigaku) with Cu Kα radiation in the 2θ range of 10°–80°. Dynamic light scattering (DLS) measurements were taken with a ...
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به خواندن ادامه دهید(a) Variation of absorbance measured at 1735 cm 1 in function of irradiation time for deposits of 20 mm thickness for homopolymers PVME and PS …
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به خواندن ادامه دهیدShimadzu 2450 – SHIMADZU spectrometer. Fourier ... PRESTIGE-2 spectrometer. Powder samples were mixed. thoroughly with KBr and pressed int o thin transp arent pellet s. X …
به خواندن ادامه دهیدFigure 7d illustrates a geopolymer sample with ratio S/L 1.75 and Na 2 SiO 3 /NaOH 1.5 and the maximum compressive strength (11.5 MPa) was obtained. For this mix design with Na 2 SiO 3 /NaOH more than 2.0, the geopolymer samples were unable to be prepared due to low workability. As such, from the figure it shows incomplete geopolymerisation due ...
به خواندن ادامه دهیدIn this study, we have focused on the synthesis, characterization and biological effects of CNSs. DLS and SEM analyses showed 50-80 nm spherical shaped CNSs with a zeta potential of …
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به خواندن ادامه دهیدThe best mix design and curing temperature by means of the highest compressive obtained after 24 h were found as NaOH: 10 M, Na4Si5O12/NaOH ratio: 0.5, Ca(OH)2: 3% (w/w), and 60 °C, respectively, which showed values of compressive strength about 10 MPa. Then early age reaction kinetics was established using Avrami–Erofe'ev model.
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